3DH7
Structure of T. thermophilus IDI-2 in complex with PPi
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM30A |
| Synchrotron site | ESRF |
| Beamline | BM30A |
| Temperature [K] | 100 |
| Wavelength(s) | 0.9797 |
| Spacegroup name | P 32 |
| Unit cell lengths | 142.528, 142.528, 109.682 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.920 - 2.970 |
| R-factor | 0.21508 |
| Rwork | 0.211 |
| R-free | 0.29254 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.032 |
| RMSD bond angle | 3.098 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.970 |
| Number of reflections | 49971 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | pH5.5, VAPOR DIFFUSION, HANGING DROP |
