3D7T

Structural basis for the recognition of c-Src by its inactivator Csk

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.1
Synchrotron site	ALS
Beamline	8.2.1
Detector technology	CCD
Spacegroup name	P 31 2 1
Unit cell lengths	99.646, 99.646, 137.058
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	45.686 - 2.899
R-factor	0.239
Rwork	0.237
R-free	0.27800
RMSD bond length	0.007
RMSD bond angle	1.148
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Refinement software	PHENIX ((phenix.refine))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.890
Number of reflections	17942
Completeness [%]	99.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP			VAPOR DIFFUSION, SITTING DROP