3D5F
Crystal Structure of PPAR-delta complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL32B2 |
| Synchrotron site | SPring-8 |
| Beamline | BL32B2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-12-20 |
| Detector | RIGAKU JUPITER 210 |
| Wavelength(s) | 1.000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 39.456, 92.829, 96.454 |
| Unit cell angles | 90.00, 98.02, 90.00 |
Refinement procedure
| Resolution | 42.470 - 2.200 |
| R-factor | 0.278 |
| Rwork | 0.278 |
| R-free | 0.28100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1gwx |
| Data reduction software | CrystalClear |
| Data scaling software | CrystalClear |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 42.470 | 2.280 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Rmerge | 0.129 | 0.416 |
| Number of reflections | 33944 | |
| <I/σ(I)> | 4.4 | 1.3 |
| Completeness [%] | 97.1 | 99.2 |
| Redundancy | 3.84 | 3.81 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6.5 | 298 | PEG 8000, pH 6.5, vapor diffusion, temperature 298K |
