Experimental procedure
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X11 |
| Temperature [K] | 298 |
| Detector technology | IMAGE PLATE |
| Collection date | 1993-11 |
| Detector | MARRESEARCH |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 62.710, 62.710, 111.090 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 8.000 - 1.600 |
| R-factor | 0.166 * |
| R-free | 0.22100 |
| Structure solution method | RIGID-BODY REFINEMENT |
| Starting model (for MR) | 2CYR |
| RMSD bond length | 0.031 |
| RMSD bond angle | 2.874 |
| Data reduction software | MOSFLM |
| Data scaling software | CCP4 ((AGROVATA) |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 38.800 | 1.680 |
| High resolution limit [Å] | 1.600 | 1.600 |
| Rmerge | 0.063 | 0.305 |
| Total number of observations | 88838 * | |
| Number of reflections | 17593 | |
| <I/σ(I)> | 8.7 | 2.4 |
| Completeness [%] | 99.1 | 98.4 |
| Redundancy | 5.1 | 4.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | other * | 4 | Matias, P.M., (1993) J. Mol. Biol., 234, 680. * |
