3CLP
M. loti cyclic-nucleotide binding domain mutant 2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X29A |
| Synchrotron site | NSLS |
| Beamline | X29A |
| Collection date | 2003-02-09 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 34.535, 82.011, 50.119 |
| Unit cell angles | 90.00, 103.64, 90.00 |
Refinement procedure
| Resolution | 48.680 - 2.000 |
| R-factor | 0.21286 |
| Rwork | 0.212 |
| R-free | 0.22938 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.221 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.300 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.038 | |
| Number of reflections | 16473 | |
| <I/σ(I)> | 8 | |
| Completeness [%] | 97.5 | 97.5 |
| Redundancy | 4 | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
