3CG1

Crystal structure of P. furiosus periplasmic binding protein ModA/WtpA with bound tungstate

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2007-09-16
Detector	PSI PILATUS 6M
Wavelength(s)	1.21340
Spacegroup name	P 1 21 1
Unit cell lengths	46.460, 109.790, 55.430
Unit cell angles	90.00, 96.22, 90.00

Refinement procedure

Resolution	30.000 - 1.600
Rwork	0.186
R-free	0.20460
Structure solution method	SAD
RMSD bond length	0.010
RMSD bond angle	1.700
Data reduction software	XDS
Data scaling software	XDS
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000
High resolution limit [Å]	1.600	1.600
Number of reflections	140430
Completeness [%]	97.7	93.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	9	293	Bicine, NaCl, PEG 600, pH 9.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K