3CFZ
Crystal structure of M. jannaschii periplasmic binding protein ModA/WtpA with bound tungstate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2007-05-18 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.21420 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.880, 89.589, 97.868 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.700 |
Rwork | 0.185 |
R-free | 0.20040 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.600 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 68998 | |
Completeness [%] | 97.4 | 93.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | Ammonium Chloride, PEG 3350, pH 7.0, VAPOR DIFFUSION |