3CDF
kI O18/O8 Y87H immunoglobulin light chain variable domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-12-11 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5241 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 72.959, 98.043, 73.074 |
Unit cell angles | 90.00, 119.60, 90.00 |
Refinement procedure
Resolution | 17.560 - 1.530 |
R-factor | 0.19118 |
Rwork | 0.189 |
R-free | 0.23147 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2q20 |
RMSD bond length | 0.019 |
RMSD bond angle | 1.858 |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.520 | 1.440 |
High resolution limit [Å] | 1.390 | 1.390 |
Number of reflections | 130900 | |
<I/σ(I)> | 14.5 | 1.9 |
Completeness [%] | 73.7 | 13.9 |
Redundancy | 3.31 | 1.82 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.1 | 295 | 1.2 M sodium citrate in 0.1 M Tris buffer, pH 8.1, VAPOR DIFFUSION, HANGING DROP, temperature 295K |