3C9D
Crystal structure of Vps75
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2007-11-05 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.9785 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.805, 86.085, 85.641 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.000 |
R-factor | 0.23 |
Rwork | 0.229 |
R-free | 0.25100 |
RMSD bond length | 0.009 |
RMSD bond angle | 0.844 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.071 | 0.408 |
Number of reflections | 37640 | |
<I/σ(I)> | 10.1 | |
Completeness [%] | 99.4 | 96.8 |
Redundancy | 4.7 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 20 mM Tris, 100 mM KCl, 10 mM MgCl(2), 35% PEG400, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |