3C80
T4 Lysozyme mutant R96Y at room temperature
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1998-11-14 |
Detector | RIGAKU RAXIS II |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 60.433, 60.433, 97.033 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.760 - 1.990 |
R-factor | 0.199 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1l63 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.216 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | TNT |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.760 | 2.100 |
High resolution limit [Å] | 1.990 | 1.990 |
Rmerge | 0.048 | 0.103 |
Number of reflections | 13030 | |
<I/σ(I)> | 27.3 | 12.8 |
Completeness [%] | 90.2 | 65.5 |
Redundancy | 6.1 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.7 | 2 M NA/K PHOSPHATE PH 6.7 550 MM NACL 50 MM REDUCED BME, 50 MM OXIDIZED BME , VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 277K, pH 6.70 |