3BKT
Copper-bound C-terminal Domain of NikR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 8-BM |
Synchrotron site | APS |
Beamline | 8-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-02-14 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9791 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.949, 78.442, 81.460 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.170 - 1.500 |
R-factor | 0.198 |
Rwork | 0.196 |
R-free | 0.22700 |
Starting model (for MR) | The tetramer of nickel-bound c-terminal domain of NikR 1q5y |
RMSD bond length | 0.011 |
RMSD bond angle | 1.346 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.059 | 0.263 |
Number of reflections | 46684 | |
<I/σ(I)> | 16.9 | 5.3 |
Completeness [%] | 97.9 | 85.2 |
Redundancy | 8.1 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 298 | 0.2M Na Tartrate, 20% PEG 3350, pH 8.0, vapor diffusion, hanging drop, temperature 298K |