3BJ9
Crystal structure of the Surrogate Light Chain Variable Domain VpreBJ
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | OXFORD DIFFRACTION ENHANCE ULTRA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-11-30 |
Detector | OXFORD |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 43.811, 67.176, 99.830 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.970 - 2.000 |
R-factor | 0.18338 |
Rwork | 0.181 |
R-free | 0.23015 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.622 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0003) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.730 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.090 | 0.235 |
Number of reflections | 9712 | |
<I/σ(I)> | 17.5 | 7.3 |
Completeness [%] | 99.4 | 92.38 |
Redundancy | 7.7 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | 0.1M Imidazole, 1M Sodium acetate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |