3BCZ
Crystal structure of Memo
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-04-01 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97990 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 139.826, 88.849, 98.089 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.970 - 2.100 |
R-factor | 0.18537 |
Rwork | 0.183 |
R-free | 0.23005 |
Structure solution method | SAD |
RMSD bond length | 0.016 |
RMSD bond angle | 1.536 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SnB |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 30.000 | 2.180 |
High resolution limit [Å] | 2.100 | 4.520 | 2.100 |
Rmerge | 0.136 | 0.072 | 0.606 |
Number of reflections | 71140 | ||
<I/σ(I)> | 7.9 | ||
Completeness [%] | 99.0 | 99.7 | 98.2 |
Redundancy | 6.6 | 6.3 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 22.5% PEG 3350, 0.1 M MES pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |