3AY8

Glutathione S-transferase unclassified 2 from Bombyx mori

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL38B1
Synchrotron site	SPring-8
Beamline	BL38B1
Temperature [K]	100
Detector technology	CCD
Detector	ADSC QUANTUM 315
Wavelength(s)	1.0000
Spacegroup name	P 32 2 1
Unit cell lengths	71.398, 71.398, 90.344
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	25.510 - 2.100
R-factor	0.18745
Rwork	0.185
R-free	0.22686
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1pn9
RMSD bond length	0.010
RMSD bond angle	1.178
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	REFMAC (5.5.0102)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.100
Number of reflections	15988
Completeness [%]	99.9
Redundancy	10

Crystallization Conditions

crystal ID	method	pH	temperature	details
1