3A0D
Crystal Structure of Polygonatum cyrtonema lectin (PCL) complexed with monomannoside
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Detector technology | IMAGE PLATE |
Collection date | 2008-02-22 |
Detector | RIGAKU RAXIS IV++ |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 76.460, 76.460, 61.750 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.160 - 2.200 |
R-factor | 0.198 |
Rwork | 0.198 |
R-free | 0.21700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3a0c |
RMSD bond length | 0.005 |
RMSD bond angle | 1.430 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.170 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.080 | 0.349 |
Number of reflections | 10885 | |
<I/σ(I)> | 4.5 | |
Completeness [%] | 99.8 | 100 |
Redundancy | 6.2 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 1.0M LiSO4, 2% PEG 8000, VAPOR DIFFUSION, HANGING DROP, temperature 293K |