399D
STRUCTURE OF D(CGCCCGCGGGCG)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ELLIOTT GX-21 |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1997-01-01 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 31.290, 42.602, 45.995 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.900 |
R-factor | 0.211 * |
Rwork | 0.165 |
R-free | 0.16800 * |
RMSD bond length | 0.010 |
RMSD bond angle | 17.103 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.000 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.042 | 0.180 |
Number of reflections | 4195 * | |
<I/σ(I)> | 11 | |
Completeness [%] | 87.5 | 79.7 |
Redundancy | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 5.6 | pH 5.60, VAPOR DIFFUSION, SITTING DROP |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | PROTEIN (PHI0) | ||
3 | 1 | 1 | NA CITRATE | ||
4 | 1 | 1 | NACL | ||
5 | 1 | 1 | AMMONIUM ACETATE | ||
6 | 1 | 1 | PEG 4000 | ||
7 | 1 | 2 | WATER | ||
8 | 1 | 2 | PEG 4000 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | duplex | 0.7 (mM) | |
2 | 1 | drop | protein | 0.5 (mM) | |
3 | 1 | drop | sodium chloride | 0.2 (M) | |
4 | 1 | drop | ammonium acetate | 0.15 (mM) | |
5 | 1 | drop | sodium citrate | 0.05 (M) | |
6 | 1 | drop | PEG4000 | 16 (%(v/v)) | |
7 | 1 | reservoir | ammonium acetate | 0.7 (M) | |
8 | 1 | reservoir | PEG4000 | 25 (%(v/v)) |