394D
CRYSTAL STRUCTURE OF TWO SELF-COMPLEMENTARY CHIMERIC DECAMERS D(CCGG)R(C)D(GCCGG) AND D(CCGG)R(CG)D(CCGG)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Detector technology | AREA DETECTOR |
Collection date | 1995-06-23 |
Detector | SIEMENS |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 25.650, 45.530, 47.930 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.900 |
R-factor | 0.177 |
Rwork | 0.177 |
RMSD bond length | 0.013 |
RMSD bond angle | 3.600 |
Data reduction software | XENGEN |
Data scaling software | XENGEN |
Refinement software | X-PLOR (3.2) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 1.900 |
Rmerge | 0.025 |
Number of reflections | 3970 |
Completeness [%] | 96.0 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 291 | pH 6.00, VAPOR DIFFUSION, HANGING DROP, temperature 291.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | NA-CACODYLATE | ||
3 | 1 | 1 | COBALT HEXAMINE | ||
4 | 1 | 1 | MPD | ||
5 | 1 | 2 | WATER | ||
6 | 1 | 2 | MPD |