365D
STRUCTURAL BASIS FOR G C RECOGNITION IN THE DNA MINOR GROOVE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Temperature [K] | 103 |
Detector technology | IMAGE PLATE |
Collection date | 1997-04-04 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 34.396, 38.959, 44.421 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 18.000 - 2.000 |
R-factor | 0.222 |
Rwork | 0.222 |
R-free | 0.26000 |
RMSD bond length | 0.030 |
RMSD bond angle | 2.200 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | X-PLOR (3.857) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 18.000 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.027 |
Number of reflections | 4124 |
Completeness [%] | 93.9 |
Redundancy | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 4 * | pH 7.50, VAPOR DIFFUSION, SITTING DROP, temperature 277.00K |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 4 * | pH 7.50, VAPOR DIFFUSION, SITTING DROP, temperature 277.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
1 | 2 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
2 | 2 | 1 | MPD | ||
3 | 1 | 1 | CA ACETATE | ||
3 | 2 | 1 | CA ACETATE | ||
4 | 1 | 1 | TRIS | ||
4 | 2 | 1 | TRIS | ||
5 | 1 | 2 | WATER | ||
5 | 2 | 2 | WATER | ||
6 | 1 | 2 | MPD | ||
6 | 2 | 2 | MPD |