35FP

Crystal structure of human Histidine Triad Nucleotide-Binding Protein 1 in complex with morpholino adenosine 6'-O-phosphate

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SEALED TUBE
Source details	RIGAKU PhotonJet-S
Temperature [K]	100
Detector technology	PIXEL
Collection date	2026-05-22
Detector	RIGAKU HyPix-6000HE
Wavelength(s)	1.54184
Spacegroup name	C 1 2 1
Unit cell lengths	67.346, 46.069, 68.192
Unit cell angles	90.00, 97.47, 90.00

Refinement procedure

Resolution	18.782 - 1.501
Rwork	0.154
R-free	0.20210
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.855
Data reduction software	CrysalisPro (1.171.44.146a)
Data scaling software	Aimless (0.8.3)
Phasing software	MOLREP (11.9.02)
Refinement software	REFMAC (5.8.0430)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	18.782	1.530
High resolution limit [Å]	1.501	1.501
Rmerge	0.052	0.340
Rpim	0.030	0.344
Number of reflections	33104	1590
<I/σ(I)>	13.4	2.1
Completeness [%]	99.3	97.7
Redundancy	3.3	2
CC(1/2)	0.998	0.722

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6	281	14% w/v PEG4000, 0.1 M MES pH 6.0