343D
STRUCTURAL PARAMETERS FROM SINGLE-CRYSTAL STRUCTURES FOR ACCURATE MODELS OF A-DNA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Temperature [K] | 298 |
| Detector technology | AREA DETECTOR |
| Collection date | 1996-02-01 |
| Detector | SIEMENS HI-STAR |
| Spacegroup name | P 1 |
| Unit cell lengths | 23.880, 33.820, 40.120 |
| Unit cell angles | 85.05, 82.91, 74.93 |
Refinement procedure
| Resolution | 8.000 - 2.100 |
| R-factor | 0.204 |
| Rwork | 0.204 |
| R-free | 0.28600 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.640 |
| Data reduction software | SAINT |
| Data scaling software | SAINT |
| Phasing software | X-PLOR |
| Refinement software | XTALVIEW |
Data quality characteristics
| Overall | |
| Rmerge | 0.051 |
| Number of reflections | 8901 |
| Redundancy | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7 | pH 7.00, VAPOR DIFFUSION |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER |
