335D
THE CRYSTAL STRUCTURE OF THE DNA DECAMER D(GGCAATTGCG) CONTAINS BOTH MAJOR AND MINOR GROOVE BINDING G.(G.C) TRIPLETS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Collection date | 1996-05-22 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 27.920, 39.210, 54.040 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.400 |
R-factor | 0.195 * |
Rwork | 0.203 |
Starting model (for MR) | PIECE OF UDJ031 |
RMSD bond length | 0.020 |
RMSD bond angle | 2.800 |
Data reduction software | DENZO |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 8.000 |
High resolution limit [Å] | 2.400 |
Rmerge | 0.080 |
Total number of observations | 1944 * |
Number of reflections | 1177 |
Completeness [%] | 96.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 * | pH 7.00, VAPOR DIFFUSION, SITTING DROP |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA | 2 (mM) | |
2 | 1 | drop | 58 (mM) | ||
3 | 1 | drop | MPD | 5 (%) | |
4 | 1 | reservoir | MPD | 30 (%) | pH7.0 |