327D
CRYSTAL STRUCTURES OF D(GM5CGM5CGCGCGC)
Experimental procedure
Source type | ROTATING ANODE |
Temperature [K] | 295 |
Detector technology | IMAGE PLATE |
Collection date | 1995-06-01 |
Detector | RIGAKU RAXIS |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 39.330, 39.330, 77.930 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 1.940 |
R-factor | 0.191 |
Rwork | 0.191 |
R-free | 0.22700 |
RMSD bond length | 0.019 |
RMSD bond angle | 2.080 |
Data reduction software | MSC |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.940 |
Rmerge | 0.052 |
Total number of observations | 12315 * |
Number of reflections | 2601 |
Completeness [%] | 86.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6 * | 22 * | VAPOR DIFFUSION |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | sodium cacodylate | 62 (mM) | |
2 | 1 | drop | DNA | 1 (mM) | single strand |
3 | 1 | drop | spermine tetrachloride | 2 (mM) | |
4 | 1 | drop | ammonium acetate | 12 (mM) | |
5 | 1 | reservoir | MPD | 75 (%(v/v)) |