Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 153 |
Detector technology | DIFFRACTOMETER |
Detector | RIGAKU AFC-5R |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 26.450, 34.660, 32.170 |
Unit cell angles | 90.00, 113.40, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.600 |
R-factor | 0.214 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.023 |
RMSD bond angle | 0.031 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 3.600 | |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 1768 | |
Completeness [%] | 75 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | VAPOR DIFFUSION, SITTING DROP, temperature 291K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | MG ACETATE | ||
4 | 1 | 1 | SPERMINE | ||
5 | 1 | 2 | WATER | ||
6 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA | 1 (mM) | |
2 | 1 | drop | magnesium acetate | 30 (mM) | |
3 | 1 | drop | spermine | 1 (M) | |
4 | 1 | drop | MPD | 10 (%(v/v)) | |
5 | 1 | reservoir | MPD | 15 (%) |