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2ZY3

dodecameric L-aspartate beta-decarboxylase

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSRRC BEAMLINE BL17B2
Synchrotron siteNSRRC
BeamlineBL17B2
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2003-07-06
DetectorRIGAKU RAXIS IV++
Wavelength(s)1.0000
Spacegroup nameC 2 2 21
Unit cell lengths149.734, 216.141, 208.726
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution50.000 - 2.500
R-factor0.178
Rwork0.175
R-free0.23400
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2zy2
RMSD bond length0.011
RMSD bond angle1.528
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.590
High resolution limit [Å]2.5002.500
Rmerge0.1210.492
Number of reflections115036
<I/σ(I)>11.22.4
Completeness [%]98.696.1
Redundancy4.34.03
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1hanging drop7.42770.1M Tris-HCl (pH 7.4), 0.1M Lithium sulfate, 15% PEG 4000, hanging drop, temperature 277K

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