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2ZWZ

alpha-L-fucosidase complexed with inhibitor, Core1

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSRRC BEAMLINE BL13C1
Synchrotron siteNSRRC
BeamlineBL13C1
Temperature [K]100
Detector technologyCCD
Collection date2007-10-09
DetectorADSC QUANTUM 210
Wavelength(s)0.97315
Spacegroup nameH 3 2
Unit cell lengths180.693, 180.693, 169.375
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution30.000 - 2.360
R-factor0.162
Rwork0.159
R-free0.21150
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)PDB enrty 1HL8
RMSD bond length0.019
RMSD bond angle1.856
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.440
High resolution limit [Å]2.3602.360
Rmerge0.0700.497
Number of reflections43077
<I/σ(I)>21.42.9
Completeness [%]99.099.7
Redundancy4.84.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.429814% PEG 5000 MME, 0.1M HEPES, pH 7.4, 4% Jeffamine M-600, VAPOR DIFFUSION, SITTING DROP, temperature 298K

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