Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

2ZSZ

Carbonmonoxy Sperm Whale Myoglobin at 100 K: Laser on [600 min]

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE AR-NW14A
Synchrotron sitePhoton Factory
BeamlineAR-NW14A
Temperature [K]100
Detector technologyCCD
Collection date2008-02-20
DetectorMAR CCD 165 mm
Wavelength(s)0.827
Spacegroup nameP 1 21 1
Unit cell lengths34.350, 30.633, 63.729
Unit cell angles90.00, 105.37, 90.00
Refinement procedure
Resolution19.940 - 1.210
R-factor0.156
Rwork0.153
R-free0.21000
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1mbc
RMSD bond length0.025
RMSD bond angle2.229
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareMOLREP
Refinement softwareREFMAC
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0001.250
High resolution limit [Å]1.2102.6101.210
Rmerge0.0520.0300.445
Number of reflections33880
<I/σ(I)>10.1
Completeness [%]85.795.527.9
Redundancy3.53.71.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1batch62932.4M Ammonium sulfate, 10mM TrisHCl, 100mM Sodium phosphate, pH 6.0, batch, temperature 293K

226707

PDB entries from 2024-10-30

PDB statisticsPDBj update infoContact PDBjnumon