2ZOW
Crystal Structure of H2O2 treated Cu,Zn-SOD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2008-03-01 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.000000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.631, 51.009, 146.990 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.940 - 1.450 |
R-factor | 0.196 |
Rwork | 0.196 |
R-free | 0.22100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ID 1Q0E |
RMSD bond length | 0.021 |
RMSD bond angle | 2.000 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.940 | 1.500 |
High resolution limit [Å] | 1.450 | 1.450 |
Number of reflections | 61462 | |
<I/σ(I)> | 3.3 | |
Completeness [%] | 99.8 | 99.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.4 | 295 | 20% (w/v) PEG 4000, 20% (w/v) iso-propanol, 0.09M MES, 1mM EDTA, pH 6.4, VAPOR DIFFUSION, SITTING DROP, temperature 295K |