2ZOI
Neutron Crystal Structure of Photoactive Yellow Protein, Wild type, at 295K
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | NUCLEAR REACTOR |
Temperature [K] | 295 |
Detector technology | IMAGE PLATE |
Collection date | 2007-03-31 |
Detector | MACSCIENCE DIP SCANNER FOR NEUTRONS |
Wavelength(s) | 2.6 |
Spacegroup name | P 63 |
Unit cell lengths | 67.145, 67.145, 41.119 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 70.000 - 1.500 |
Rwork | 0.192 |
R-free | 0.21900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zoh |
RMSD bond length | 0.013 |
RMSD bond angle | 1.700 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.109 | 0.324 |
Number of reflections | 15293 | |
<I/σ(I)> | 7.4 | 2.91 |
Completeness [%] | 89.6 | 72.8 |
Redundancy | 2.6 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP, MICROSEEDING | 9 | 295 | AMMONIUM SULPHATE, SODIUM CHLORIDE, SODIUM DIDEUTERIUM PHOSPHATE, DISODIUM DEUTERIUM PHOSPHATE, pH 9.0, VAPOR DIFFUSION, HANGING DROP, MICROSEEDING, temperature 295K |