2ZNZ
Crystal structure of FFRP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2007-10-17 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.000 |
Spacegroup name | P 1 2 1 |
Unit cell lengths | 98.230, 102.340, 104.050 |
Unit cell angles | 90.00, 118.05, 90.00 |
Refinement procedure
Resolution | 46.300 - 2.390 |
R-factor | 0.206 |
Rwork | 0.206 |
R-free | 0.20900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ri7 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.480 |
High resolution limit [Å] | 2.390 | 2.390 |
Rmerge | 0.087 | 0.230 |
Number of reflections | 71303 | |
<I/σ(I)> | 17.47 | 4.83 |
Completeness [%] | 99.6 | 99.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 294 | 20% PEG 3350, 0.3M CaCl2, pH 7, VAPOR DIFFUSION, SITTING DROP, temperature 294K |