2ZLU
Horse methemoglobin high salt, pH 7.0 (88% relative humidity)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 2003-04-15 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 108.184, 63.336, 54.409 |
Unit cell angles | 90.00, 111.09, 90.00 |
Refinement procedure
Resolution | 19.980 - 2.000 |
R-factor | 0.19471 |
Rwork | 0.193 |
R-free | 0.22150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2mhb |
RMSD bond length | 0.014 |
RMSD bond angle | 1.318 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.106 | 0.445 |
Number of reflections | 22583 | |
<I/σ(I)> | 7.3 | 2.5 |
Completeness [%] | 96.8 | |
Redundancy | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIQUID DIFFUSION | 7 | 298 | 2.6M ammonium sulfate, 0.01M ammonium phosphate, pH 7.0, LIQUID DIFFUSION, temperature 298.0K |