Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-07-09 |
Detector | RIGAKU RAXIS V |
Wavelength(s) | 0.9 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 62.306, 62.306, 185.532 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 1.150 |
Rwork | 0.098 |
R-free | 0.13590 |
Structure solution method | AB INITIO |
RMSD bond length | 0.030 |
RMSD bond angle | 0.031 |
Phasing software | SHELX |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.150 |
Number of reflections | 76207 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | 0.1M sodium citrate, 1M Ammonium Phosphate , pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |