2ZJ2
Archaeal DNA helicase Hjm apo state in form 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-02-06 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9790 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 117.269, 83.441, 95.019 |
Unit cell angles | 90.00, 120.69, 90.00 |
Refinement procedure
Resolution | 44.860 - 2.400 |
R-factor | 0.228 |
Rwork | 0.228 |
R-free | 0.29900 |
Structure solution method | MIR |
RMSD bond length | 0.008 |
RMSD bond angle | 1.300 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.086 | 0.375 |
Number of reflections | 30454 | |
<I/σ(I)> | 11.2 | |
Completeness [%] | 98.2 | 92.1 |
Redundancy | 5.6 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 1.6M Ammonium suflate, 0.1M citrate, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |