2ZIU
Crystal structure of the Mus81-Eme1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 4A |
Synchrotron site | PAL/PLS |
Beamline | 4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-03-02 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 88.681, 88.681, 170.216 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.030 - 2.700 |
R-factor | 0.234 |
Rwork | 0.234 |
R-free | 0.28600 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.007 |
RMSD bond angle | 1.300 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.830 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.090 | 0.313 |
Number of reflections | 27255 | |
<I/σ(I)> | 41.3 | 6.6 |
Completeness [%] | 99.6 | 99.7 |
Redundancy | 15.8 | 13.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 277 | 0.1M Na-Acetate, 2.3M Ammonium chlorede, pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |