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2ZHM

Crystal structure of human galectin-9 N-terminal CRD in complex with N-acetyllactosamine trimer (crystal 1)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE AR-NW12A
Synchrotron sitePhoton Factory
BeamlineAR-NW12A
Temperature [K]100
Detector technologyCCD
Collection date2006-02-17
DetectorADSC QUANTUM 210
Spacegroup nameP 21 21 21
Unit cell lengths35.217, 67.964, 219.964
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution36.900 - 1.840
R-factor0.185
Rwork0.182
R-free0.23500
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.012
RMSD bond angle1.408
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]36.9001.920
High resolution limit [Å]1.8401.850
Number of reflections45532
Completeness [%]98.999.5
Redundancy10.911.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.2293200MM AMMONIUM FLUORIDE, 20% PEG 3350, pH 6.20, VAPOR DIFFUSION, SITTING DROP, temperature 293K

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