2ZGS
Crystal structure of Agrocybe aegerita lectin AAL mutant L47A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 98 |
Detector technology | IMAGE PLATE |
Collection date | 2007-08-21 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.250, 65.930, 57.950 |
Unit cell angles | 90.00, 109.09, 90.00 |
Refinement procedure
Resolution | 24.480 - 1.900 |
R-factor | 0.208 |
Rwork | 0.208 |
R-free | 0.24000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zgl |
RMSD bond length | 0.006 |
RMSD bond angle | 1.500 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.490 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.063 | 0.300 |
Number of reflections | 29971 | |
<I/σ(I)> | 19.3 | 4.1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 4 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | 0.2M Sodium Chloride, 20% PEG3350, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |