2ZGR
Crystal structure of AAL mutant L33A in C2 spacegroup
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 98 |
Detector technology | IMAGE PLATE |
Collection date | 2005-08-01 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 58.190, 49.270, 50.380 |
Unit cell angles | 90.00, 102.19, 90.00 |
Refinement procedure
Resolution | 24.640 - 1.900 |
R-factor | 0.214 |
Rwork | 0.214 |
R-free | 0.24600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zgl |
RMSD bond length | 0.005 |
RMSD bond angle | 1.400 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.640 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.048 | 0.275 |
Number of reflections | 13022 | |
<I/σ(I)> | 21.4 | 3.7 |
Completeness [%] | 100.0 | 100 |
Redundancy | 3.5 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.8 | 298 | 2M Ammonium Sulfate, pH 5.8, VAPOR DIFFUSION, HANGING DROP, temperature 298K |