2ZBT
Crystal structure of pyridoxine biosynthesis protein from Thermus thermophilus HB8
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B2 |
Synchrotron site | SPring-8 |
Beamline | BL26B2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-12-09 |
Detector | RIGAKU JUPITER 210 |
Wavelength(s) | 0.97904, 0.9000, 0.97942 |
Spacegroup name | H 3 |
Unit cell lengths | 180.970, 180.970, 100.750 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.960 - 1.650 |
R-factor | 0.194 |
Rwork | 0.194 |
R-free | 0.21000 |
Structure solution method | MAD |
RMSD bond length | 0.005 |
RMSD bond angle | 1.400 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.710 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.040 | 0.221 |
Number of reflections | 148066 | |
<I/σ(I)> | 52.73 | 6.2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.4 | 6.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.7 | 293 | 0.1M Magnesium acetate, 0.1M Sodium cacodylate pH6.7, 22.5% MPD, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
1 | VAPOR DIFFUSION, SITTING DROP | 6.7 | 293 | 0.1M Magnesium acetate, 0.1M Sodium cacodylate pH6.7, 22.5% MPD, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
1 | VAPOR DIFFUSION, SITTING DROP | 6.7 | 293 | 0.1M Magnesium acetate, 0.1M Sodium cacodylate pH6.7, 22.5% MPD, VAPOR DIFFUSION, SITTING DROP, temperature 293K |