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2Z18

Phase transition of monoclinic lysozyme crystal soaked in a 10% NaCl solution

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsMACSCIENCE
Temperature [K]90
Detector technologyCCD
Collection date2006-12-11
DetectorBRUKER SMART 6000
Wavelength(s)1.5418
Spacegroup nameP 1 21 1
Unit cell lengths26.622, 60.588, 31.223
Unit cell angles90.00, 111.44, 90.00
Refinement procedure
Resolution25.000 - 1.150
Rwork0.156
R-free0.17600
Structure solution methodSHELX-97
Starting model (for MR)2d4j
RMSD bond length0.012
RMSD bond angle0.029
Data reduction softwareSAINT (Plus)
Data scaling softwareSAINT (Plus)
Phasing softwareSHELXL-97
Refinement softwareSHELXL-97
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.190
High resolution limit [Å]1.1501.150
Rmerge0.1040.090
Number of reflections32729
Completeness [%]99.699.9
Redundancy4.733.09
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Dehydration induced phase transition29310% NaCl, temperature-regulated nitrogen gas, Dehydration induced phase transition, temperature 293K

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