2Z0F
Crystal structure of putative phosphoglucomutase from Thermus thermophilus HB8
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B1 |
Synchrotron site | SPring-8 |
Beamline | BL26B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-12-23 |
Detector | RIGAKU JUPITER 210 |
Wavelength(s) | 0.9793, 1.0000, 0.9796 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 80.676, 102.297, 87.462 |
Unit cell angles | 90.00, 117.19, 90.00 |
Refinement procedure
Resolution | 19.910 - 2.520 |
R-factor | 0.206 |
Rwork | 0.206 |
R-free | 0.25700 |
Structure solution method | MAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.300 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 41420 | |
<I/σ(I)> | 20 | 3.3 |
Completeness [%] | 97.8 | 86.2 |
Redundancy | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.6 | 293 | 12% PEG6000, 0.2M Lithium Sulfate, 0.1M Na3 Citrate, pH 5.6, temperature 293K |