2YPG
Haemagglutinin of 1968 Human H3N2 Virus in Complex with Human Receptor Analogue LSTc
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2012-02-13 |
Detector | ADSC CCD |
Spacegroup name | P 41 |
Unit cell lengths | 160.767, 160.767, 177.210 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 160.770 - 2.850 |
R-factor | 0.17771 |
Rwork | 0.177 |
R-free | 0.19036 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.462 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 177.210 |
High resolution limit [Å] | 2.850 |
Rmerge | 0.130 |
Number of reflections | 104897 |
<I/σ(I)> | 11.2 |
Completeness [%] | 100.0 |
Redundancy | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 1.7-2 M TRIAMMONIUM CITRATE PH 6.5 |