Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | LNLS BEAMLINE W01B-MX2 |
| Synchrotron site | LNLS |
| Beamline | W01B-MX2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARMOSAIC 225 mm CCD |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 56.734, 69.187, 90.569 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 39.480 - 1.670 |
| R-factor | 0.13048 |
| Rwork | 0.129 |
| R-free | 0.16057 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1cel |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.483 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 45.300 |
| High resolution limit [Å] | 1.670 |
| Rmerge | 0.090 |
| Number of reflections | 42070 |
| <I/σ(I)> | 24.4 |
| Completeness [%] | 99.8 |
| Redundancy | 6.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 25% PEG 4000 AND 5 MM CACL2 |
