2YLB
Structure of Salmonella typhimurium Hfq at 1.15 A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 2009-05-19 |
Detector | MARRESEARCH |
Spacegroup name | P 61 |
Unit cell lengths | 61.400, 61.400, 167.030 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 18.840 - 1.150 |
R-factor | 0.1701 |
Rwork | 0.168 |
R-free | 0.20760 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1hk9 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.614 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.180 |
High resolution limit [Å] | 1.150 | 1.150 |
Number of reflections | 123284 | |
<I/σ(I)> | 12.8 | 2.52 |
Completeness [%] | 98.0 | 96.9 |
Redundancy | 4.9 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 0.1 M HEPES (PH=7.0), 0.5 % JEFFAMINE, 1.1 M MALONATE |