2YL1
CYTOCHROME C PRIME FROM ALCALIGENES XYLOSOXIDANS: CARBON MONOOXIDE BOUND L16A VARIANT AT 1.03 A RESOLUTION - Restraint refinement
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2009-06-04 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 53.009, 53.009, 181.114 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.240 - 1.030 |
R-factor | 0.13386 |
Rwork | 0.133 |
R-free | 0.14271 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2yl0 |
RMSD bond length | 0.018 |
RMSD bond angle | 1.935 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.540 | 1.090 |
High resolution limit [Å] | 1.030 | 1.030 |
Rmerge | 0.070 | 0.710 |
Number of reflections | 75580 | |
<I/σ(I)> | 12.7 | 2.5 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 7.8 | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | AMMONIUM SULPHATE, TRIS PH 7.5 |