2YKI
Tricyclic series of Hsp90 inhibitors
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | NONIUS |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2005-04-21 |
Detector | MAR scanner 345 mm plate |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 66.622, 90.562, 99.104 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.035 - 1.670 |
R-factor | 0.239 |
Rwork | 0.239 |
R-free | 0.25800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.210 |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 21.030 |
High resolution limit [Å] | 1.670 |
Rmerge | 0.090 |
Number of reflections | 35143 |
Completeness [%] | 95.8 |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.5 |