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2YJX

Tricyclic series of Hsp90 inhibitors

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007 HF
Temperature [K]100
Detector technologyCCD
Collection date2010-11-09
DetectorMARRESEARCH
Spacegroup nameI 2 2 2
Unit cell lengths66.399, 90.765, 98.734
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution23.550 - 1.830
R-factor0.1761
Rwork0.175
R-free0.19860
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.010
RMSD bond angle1.020
Data reduction softwarePROCESS-XDS
Data scaling softwareSCALA
Phasing softwareAMoRE
Refinement softwareBUSTER (2.9.7)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]23.5501.910
High resolution limit [Å]1.8301.830
Rmerge0.0400.210
Number of reflections26359
Completeness [%]99.697.5
Redundancy6.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
17.5pH 7.5

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PDB entries from 2024-11-06

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