2YJK
Structure of Dps from MICROBACTERIUM ARBORESCENS in the high iron form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 87.580, 92.050, 128.580 |
Unit cell angles | 90.00, 96.04, 90.00 |
Refinement procedure
Resolution | 28.980 - 2.000 |
R-factor | 0.17227 |
Rwork | 0.170 |
R-free | 0.21650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1o9r |
RMSD bond length | 0.025 |
RMSD bond angle | 1.821 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.100 | 0.880 |
Number of reflections | 129605 | |
<I/σ(I)> | 7.3 | 1.5 |
Completeness [%] | 98.0 | 96.8 |
Redundancy | 2.05 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 18% PEG 8000, 2% ISO-PROPANOL, 0.1 M NA-ACETATE, PH 7.5. |