2YGO
WIF domain-EGF-like domain 1 of human Wnt inhibitory factor 1 in complex with 1,2-dipalmitoylphosphatidylcholine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 50.996, 134.260, 60.403 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.422 - 1.850 |
R-factor | 0.1856 |
Rwork | 0.184 |
R-free | 0.21680 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 2.069 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.990 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.140 | 0.940 |
Number of reflections | 18293 | |
<I/σ(I)> | 15.5 | 1.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.3 | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 1.3 M DIAMMONIUM TARTRATE, 100 MM BIS-TRIS PROPANE PH 7.0 |