Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX10.1 |
| Synchrotron site | SRS |
| Beamline | PX10.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | F 4 3 2 |
| Unit cell lengths | 191.801, 191.801, 191.801 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 36.910 - 1.800 |
| R-factor | 0.16448 |
| Rwork | 0.164 |
| R-free | 0.18032 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2yfu |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.292 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.000 | 1.900 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.110 | 0.540 |
| Number of reflections | 28579 | |
| <I/σ(I)> | 18.2 | 4.6 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 10.5 | 10.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.8 | 0.2 M TRI-SODIUM CITRATE, PH 4.8 . |
