2YDG
Ascorbate co-crystallized HEWL.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-05-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.939 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.770, 78.770, 37.370 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.790 - 2.000 |
R-factor | 0.15501 |
Rwork | 0.152 |
R-free | 0.18648 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2w1l |
RMSD bond length | 0.014 |
RMSD bond angle | 1.689 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 2.440 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.050 | 0.070 |
Number of reflections | 8387 | 3693 |
<I/σ(I)> | 8.7 | 8.6 |
Completeness [%] | 99.8 | 99.9 |
Redundancy | 6.6 | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.7 | 293 | 200 MM SODIUM ACETATE BUFFER AT PH 4.7 CONTAINING 10 % W/V NACL. |