2YDF
HUMAN SERUM ALBUMIN COMPLEXED WITH IOPHENOXIC ACID
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX14.1 |
| Synchrotron site | SRS |
| Beamline | PX14.1 |
| Temperature [K] | 298 |
| Detector technology | CCD |
| Collection date | 2007-12-15 |
| Detector | ADSC QUANTUM 4 |
| Spacegroup name | P 1 |
| Unit cell lengths | 55.072, 55.440, 119.845 |
| Unit cell angles | 81.00, 90.83, 64.52 |
Refinement procedure
| Resolution | 35.124 - 2.750 |
| R-factor | 0.2081 |
| Rwork | 0.207 |
| R-free | 0.23930 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2bxa |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.599 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | CNS |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 59.000 | 2.900 |
| High resolution limit [Å] | 2.750 | 2.750 |
| Rmerge | 0.090 | 0.340 |
| Number of reflections | 31655 | |
| <I/σ(I)> | 8.2 | 1.7 |
| Completeness [%] | 95.5 | 92.9 |
| Redundancy | 1.9 | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | SEE PAPER, pH 7 |
